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Nanoscale Depth Profiling of Residual Stresses Due to Fine Surface Finishing

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Mechanical polishing is commonly used for both surface finishing and metallographic sample preparation for a broad range of materials. However, polishing causes local deformation and induces residual stress, which has… Click to show full abstract

Mechanical polishing is commonly used for both surface finishing and metallographic sample preparation for a broad range of materials. However, polishing causes local deformation and induces residual stress, which has an important effect on many surface phenomena. Until recently, it has not been possible to quantify the nanoscale depth variation of polishing-induced plastic deformation (eigenstrain) and the associated residual stress. In this study, the magnitude and depth of polishing-induced residual stress are evaluated directly for the first time, by focused ion beam milling and digital image correlation using a micro-ring-core geometry (FIBDIC method). Depth-resolved residual stress profiles are obtained with submicron resolution at the surface of a titanium alloy sample that was subjected to various polishing steps. It is found that electrochemical polishing and polishing with colloidal silica does not induce any significant residual stress. However, polishing with diamond slurry leads to the formation of compressive residual stresses of up to 300 MPa, which extend deeper into the material when larger diamond particles are used. This study paves the way for further research on polishing and its effect on surface properties.

Keywords: depth; surface; residual stress; surface finishing; nanoscale depth

Journal Title: Advanced Materials Interfaces
Year Published: 2019

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