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Electrochemical Direct Thiolation of Lactams with Mercaptans: An Efficient Access to N-Acylsulfenamides

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A variety of N‐acylsulfenamides are produced by the electrochemically enabled cross‐coupling of readily available feedstocks under standard conditions. This protocol is practical and has wide substrate scope with good reaction… Click to show full abstract

A variety of N‐acylsulfenamides are produced by the electrochemically enabled cross‐coupling of readily available feedstocks under standard conditions. This protocol is practical and has wide substrate scope with good reaction efficiency (38 examples, up to 97 % yield). A possible free radical mechanism is preliminarily demonstrated.

Keywords: thiolation lactams; lactams mercaptans; mercaptans efficient; electrochemical direct; efficient access; direct thiolation

Journal Title: European Journal of Organic Chemistry
Year Published: 2021

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