A facile and efficient two-step synthetic route to previously inaccessible 1,3-unsubstituted 2-imino-5-oxooctahydroimidazo[4,5-d]-imidazol-1-ium iodides has been developed using easily accessible thioglycolurils, MeI, and various primary amines, morpholine, or ethylene diamine. The… Click to show full abstract
A facile and efficient two-step synthetic route to previously inaccessible 1,3-unsubstituted 2-imino-5-oxooctahydroimidazo[4,5-d]-imidazol-1-ium iodides has been developed using easily accessible thioglycolurils, MeI, and various primary amines, morpholine, or ethylene diamine. The structure of representative products and hydrogen-bonding pattern in their crystals have been investigated by X-ray diffraction.
Keywords:
unsubstituted imino;
efficient method;
imino oxooctahydroimidazo;
method synthesis
Journal Title: Chemistry of Heterocyclic Compounds
Year Published: 2019
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Journal Title: Chemistry of Heterocyclic Compounds
Year Published: 2019
Link to full text (if available)
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recommendations!