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A convenient and inexpensive approach for the synthesis of deuterium-labeled thiamphenicol was described. DL-threo-Thiamphenicol-methyl-d3 was prepared with high chemical purity and isotopic enrichment via a six-step process starting from 4-bromobenzaldehyde… Click to show full abstract
A convenient and inexpensive approach for the synthesis of deuterium-labeled thiamphenicol was described. DL-threo-Thiamphenicol-methyl-d3 was prepared with high chemical purity and isotopic enrichment via a six-step process starting from 4-bromobenzaldehyde and DMSO-d6 by employing microwave-assisted copper-mediated methylthiolation and modified Wulff’s asymmetric aziridination.
Keywords:
deuterium labeled;
thiamphenicol;
synthesis deuterium;
threo thiamphenicol
Journal Title: Journal of Radioanalytical and Nuclear Chemistry
Year Published: 2020
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Journal Title: Journal of Radioanalytical and Nuclear Chemistry
Year Published: 2020
Link to full text (if available)
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recommendations!