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A reaction of Bu4N[8,8´-(MeS)2-3,3´-Co(1,2-C2B9H10)2] with (MeCN)3W(CO)3 in dichloromethane gave a mixture of Bu4N{(CO)5W[κ-8,8´-(MeS)2-3,3´-Co(1,2-C2B9H10)2]} and Bu4N{[(CO)5W]2[κ2-8,8´-(MeS)2-3,3´-Co(1,2-C2B9H10)2]}, which were separated by column chromatography on silica gel. Click to show full abstract
A reaction of Bu4N[8,8´-(MeS)2-3,3´-Co(1,2-C2B9H10)2] with (MeCN)3W(CO)3 in dichloromethane gave a mixture of Bu4N{(CO)5W[κ-8,8´-(MeS)2-3,3´-Co(1,2-C2B9H10)2]} and Bu4N{[(CO)5W]2[κ2-8,8´-(MeS)2-3,3´-Co(1,2-C2B9H10)2]}, which were separated by column chromatography on silica gel.
Keywords:
cobalt bis;
bu4n mes;
methylthio dicarbollide;
bis methylthio;
synthesis cobalt;
mes c2b9h10
Journal Title: Russian Chemical Bulletin
Year Published: 2018
Link to full text (if available)
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Journal Title: Russian Chemical Bulletin
Year Published: 2018
Link to full text (if available)
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recommendations!