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In this work, we report the synthesis, characterization, crystal structure, and thermal and antibacterial studies of a new nano-sized copper(I) thiosemicarbazone complex prepared by an ultrasonic bath assisted synthesis in… Click to show full abstract
In this work, we report the synthesis, characterization, crystal structure, and thermal and antibacterial studies of a new nano-sized copper(I) thiosemicarbazone complex prepared by an ultrasonic bath assisted synthesis in an acetonitrile solution. Characterization of the complex and its ligand (EHB-tsc = 3-ethoxy-4-hydroxybenzaldehyde-thiosemicarbazone) was performed using elemental analysis, FT-IR, 1H and 13C-NMR, UV–Vis spectroscopy, thermal gravimetry, and single-crystal X-ray diffraction. In addition, the complex was characterized by X-ray powder diffraction and scanning electron microscopy.
Journal Title: Journal of the Iranian Chemical Society
Year Published: 2019
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