Abstract The aim of this paper is to investigate the effect of slip casting process and the annealing before and after sintering to achieve a transparent MgAl2O4. To remove contaminants… Click to show full abstract
Abstract The aim of this paper is to investigate the effect of slip casting process and the annealing before and after sintering to achieve a transparent MgAl2O4. To remove contaminants such as carbon from the structure of shaped spinel bodies, at first, the samples were annealed at temperature of 800 °C, 900 °C and 1000 °C for 2 h and then sintered at 1400 °C. By annealing the sample before sintering at 900 °C, the transmission increased (15% at IR region and 10% at visible region). Although by annealing the samples, the amount of carbon contamination reduced. Annealing the samples after sintering also had some desirable results. The samples annealed at temperature of 1200 °C for a time of 3, 5 and 10 h. The darkness of samples reduced due to the removal of carbon impurities and the sample was annealed at 1200 °C for 5 h had the most transparency in the visible and infrared regions.
               
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