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Fabrication and mechanical properties of porous Si3N4 ceramics prepared via SHS

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Abstract Porous silicon nitride ceramics were directly prepared by self-propagating high temperature synthesis (SHS). The effects of Si 3 N 4 diluent and Y 2 O 3 sintering additive on… Click to show full abstract

Abstract Porous silicon nitride ceramics were directly prepared by self-propagating high temperature synthesis (SHS). The effects of Si 3 N 4 diluent and Y 2 O 3 sintering additive on the phase composition and microstructure were investigated. The XRD patterns and SEM microstructures proved the sample with 63 wt% Si 3 N 4 diluent could provide appropriate temperature, reaction time and porosity for the fabrication of elongated β-Si 3 N 4 porous ceramics. A porosity of 40%–47% and a flexural strength of 118–216 MPa were obtained after SHS with different Y 2 O 3 content. Besides, the excellent thermal shock resistance of Si 3 N 4 assured that strength retention keeps stable in the temperature difference ( Δ T) of 800 °C.

Keywords: fabrication; mechanical properties; si3n4 ceramics; properties porous; fabrication mechanical; porous si3n4

Journal Title: Ceramics International
Year Published: 2019

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