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Effect of a glaze layer on adhesion energy between resin cements to zirconia ceramic

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Abstract Purpose To evaluate the effect of an etched and silanized glazed porcelain layer on the interfacial fracture toughness between a zirconia ceramic and resin cements. Materials and methods Forty… Click to show full abstract

Abstract Purpose To evaluate the effect of an etched and silanized glazed porcelain layer on the interfacial fracture toughness between a zirconia ceramic and resin cements. Materials and methods Forty rectangular-shaped yttrium stabilised zirconia ceramic plates were sintered and sandblasted with 100 µm Al2O3. Twenty specimens were glazed with Akzent Glaze Spray and then etched with 9% hydrofluoric acid for 3 min prior to being silanized with Monobond-S. Glazed and non-glazed specimens were further divided into two groups (n = 10) and allocated to one of two resin bonding systems, Variolink II and Multilink-Automix (Ivoclar Vivadent). The Multilink-Automix groups were treated with Metal/Zirconia Primer. Glass rods (12 mm) were bonded to each prepared zirconia plate, using the two bonding systems and were loaded to failure using a universal testing machine. Strain energy release rate (bond) values were calculated and de-bonded specimens were examined using SEM to determine the modes of failure. Data were analysed using two-tailed T-test and Dunnett-T3 post-hoc tests with statistical significance set at p Results Glazed zirconia surface significantly improved the mean bond values in the Variolink II group (p 0.05) in the Multilink-Automix Metal/Zirconia Primer group; the Multilink – Automix group, produced significantly higher bond values in the non-glazed group (p Conclusion Glazed zirconia surfaces produced higher resin cement bond strength than unglazed zirconia, however the combination of silanised phosphate monomer and metal/zirconia primer produced weaker bond on glazed zirconia.

Keywords: resin; zirconia ceramic; multilink automix; bond; zirconia; resin cements

Journal Title: International Journal of Adhesion and Adhesives
Year Published: 2018

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