Abstract Mesoporous manganese oxide was prepared by a non-ionic surfactant route using Triton X-100, followed by Ag nanoparticle (NP) and graphene oxide incorporation by an ultra-sonication-assisted process. Fine Ag NPs… Click to show full abstract
Abstract Mesoporous manganese oxide was prepared by a non-ionic surfactant route using Triton X-100, followed by Ag nanoparticle (NP) and graphene oxide incorporation by an ultra-sonication-assisted process. Fine Ag NPs were incorporated into the tubular texture of mesoporous manganese oxide. The crystalline phase, particle size, and morphology of the prepared materials were characterized by X-ray diffraction (XRD), Barrett–Joyner–Halenda–Brunauer–Emmett–Teller analysis, scanning electron microscopy–energy dispersive X-ray analysis, and high-resolution transmission electron microscopy (HR-TEM). The XRD results confirmed the formation of the Mn2O3 phase for the as-prepared mesoporous manganese oxide and its nanocomposite. Very fine Ag NPs ( 98% removal of Cr(VI) within 1–2 h of reaction time) for Ag NP-incorporated mesoporous MnO2. Efficient activity was observed because of the fine Ag NPs present in mesoporous manganese oxide, as opposed to the case of graphene oxide-doped meso-MnO2 and pristine mesoporous meso-MnO2.
               
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