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Electrically-activated reactive synthesis (EARS) and electro-annealing of Ni/CNT-Al nanocomposite powders

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Abstract The present paper discusses the electrically activated reactive synthesis (EARS) of Ni/CNT-Al nano-composite powders. The effect of initial relative green density (RGD) on reaction characteristics and resultant microstructure has… Click to show full abstract

Abstract The present paper discusses the electrically activated reactive synthesis (EARS) of Ni/CNT-Al nano-composite powders. The effect of initial relative green density (RGD) on reaction characteristics and resultant microstructure has been investigated in addition to post reaction electro-annealing. Results show that a relative density of 0.67 RGD resulted in the highest combustion temperature and lowest product porosity, while detrimental cracking was observed at the higher RGDs during EARS. Post reaction electro-annealing was also found to promote homogenization and sintering of as-reacted products. Microhardness values as high as ∼250 HV are reported following electro-annealing.

Keywords: activated reactive; electrically activated; synthesis ears; electro annealing; reactive synthesis

Journal Title: Journal of Alloys and Compounds
Year Published: 2019

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