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Synthesis of spherical and cubic magnetic iron oxide nanocrystals at low temperature in air.

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Synthesis of magnetite nanocrystals typically requires harsh reaction conditions, including high reaction pressures and/or temperatures, to obtain morphology-controlled nanocrystals like cubic magnetite nanocrystals. We report the synthesis of cubic magnetite… Click to show full abstract

Synthesis of magnetite nanocrystals typically requires harsh reaction conditions, including high reaction pressures and/or temperatures, to obtain morphology-controlled nanocrystals like cubic magnetite nanocrystals. We report the synthesis of cubic magnetite nanocrystals with a size of 9 nm at reaction temperatures less than 100 °C in air. The synthesized magnetite nanocubes exhibited uniform size and highly crystalline nature. In addition, we synthesized size-controlled spherical magnetite nanocrystals in the size range of 2.5 nm to 9 nm by modifying the reaction conditions.

Keywords: synthesis spherical; magnetite nanocrystals; air; size; reaction; synthesis

Journal Title: Journal of colloid and interface science
Year Published: 2018

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