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In-situ electrochemical oxide monitoring in LiF-NdF3-Nd2O3: Application to Nd2O3 solubility determination

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Abstract Neodymium oxide titration was investigated in the LiF-NdF3-Nd2O3 melt on platinum electrode by square wave voltammetry (SWV) in order to develop an in-situ and fast technique for oxide amount… Click to show full abstract

Abstract Neodymium oxide titration was investigated in the LiF-NdF3-Nd2O3 melt on platinum electrode by square wave voltammetry (SWV) in order to develop an in-situ and fast technique for oxide amount monitoring during Nd or Nd-Fe production by electrolysis. The methodology was verified by elemental analyses in the 850–1050 °C temperature range and then applied to Nd2O3 solubility determination in LiF-NdF3.

Keywords: ndf3 nd2o3; nd2o3 solubility; lif ndf3; solubility determination

Journal Title: Journal of Electroanalytical Chemistry
Year Published: 2021

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