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New insight into the microstructure–thermal stability relationships in ceria-zirconia solid solution and the application in Pd-only three-way catalyst

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Abstract Three ceria-zirconia solid solutions were prepared by different synthesis routes. The results showed that CZ3 exhibited incompact structure with heterogeneous particle size distribution, accompanied by a bimodal pore size… Click to show full abstract

Abstract Three ceria-zirconia solid solutions were prepared by different synthesis routes. The results showed that CZ3 exhibited incompact structure with heterogeneous particle size distribution, accompanied by a bimodal pore size distribution. After aging treatment, the specific surface area and cumulative pore volume of CZ3-a were 37 m2/g and 0.22 cm3/g, which decreased by only 51% and 4% respectively from the fresh state. And the particle volume increased by only 4 times. Among the three samples, the textural/structural properties of CZ3 showed the smallest degradation, indicating the highest thermal stability, which was attributed to the incompact structure and special texture.

Keywords: zirconia solid; ceria zirconia; new insight; insight microstructure; thermal stability

Journal Title: Journal of Industrial and Engineering Chemistry
Year Published: 2017

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