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Microstructural stability of in-situ TiB2/Al composite during solution treatment

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Abstract The microstructural stability including grain growth and texture of in-situ TiB 2 /Al composite during solution treatment (ST) at T4 state (natural aging) was investigated for the first time.… Click to show full abstract

Abstract The microstructural stability including grain growth and texture of in-situ TiB 2 /Al composite during solution treatment (ST) at T4 state (natural aging) was investigated for the first time. The results show that the nano TiB 2 particles have a strong influence on the stability of grain size (GS) and textures during ST. The composite has exhibited improved stability of GS attributing to the Zener pinning of TiB 2 particles, resulting in no obvious increase in GS after the ST for 24 h. A modified Zener equation has been proposed for the composite with non-uniform particle distribution, which can make a good prediction on the limiting GS. For textures of the 2024 alloy and TiB 2 /2024 composite, there is not much difference in the intensity of 〈111〉 fiber before the ST, while the 〈l00〉 fiber is stronger in the composite. The 〈111〉 and 〈l00〉 double fibers of the composite are stabilized by TiB 2 particles during ST at T4 state. However, the 〈111〉 and 〈100〉 fibers of the alloy are gradually replaced by 〈113〉, 〈102〉 and 〈302〉 ones due to the recrystallization and grain growth. Accordingly, the composite exhibits much stronger fiber textures than the alloy after the heat treatment.

Keywords: solution treatment; treatment; composite solution; situ; stability; microstructural stability

Journal Title: Materials Characterization
Year Published: 2017

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