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Synthesis and characterisation of titanium dioxide nanoparticles prepared within hyperbranched polyethylenimine polymer template using a modified sol–gel method

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Templated synthesis of nanoparticles has been shown to result in uniform sized and well dispersed particles. Titanium dioxide (TiO2) nanoparticles were prepared through a modified sol–gel method using hyperbranched polyethyleneimine… Click to show full abstract

Templated synthesis of nanoparticles has been shown to result in uniform sized and well dispersed particles. Titanium dioxide (TiO2) nanoparticles were prepared through a modified sol–gel method using hyperbranched polyethyleneimine (HPEI) as a template to reduce their agglomeration. The synthesised HPEI/TiO2 nanocomposites were characterised by techniques such as Transmission Electron microscopy (TEM), Fourier Transform Infrared spectroscopy (FTIR), Powder-X-ray Diffraction spectroscopy (XRD) and Thermo-gravimetric analysis (TGA). TEM micrographs illustrated formation of small and well dispersed TiO2nanoparticles. The use of HPEI therefore had a huge impact on the size, shape and dispersion of theTiO2 nanoparticles.

Keywords: modified sol; titanium dioxide; spectroscopy; nanoparticles prepared; sol gel; gel method

Journal Title: Materials Letters
Year Published: 2017

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