Abstract The half-Heusler thermoelectric bulks Zr x Ti 1−x NiSn (x = 0.1, 0.2, 0.3, 0.4) were rapidly prepared by microwave heating. The phase composition and microstructure were characterized by X-ray diffractometer… Click to show full abstract
Abstract The half-Heusler thermoelectric bulks Zr x Ti 1−x NiSn (x = 0.1, 0.2, 0.3, 0.4) were rapidly prepared by microwave heating. The phase composition and microstructure were characterized by X-ray diffractometer (XRD) and scanning electron microscopy (SEM). The electrical and thermal properties were measured by Seebeck coefficient/resistance analysis system (S/RAs) and laser flash thermal analyzer (LFT). The point defects came from Zr-substitution and the in-situ nanostructure attributed to microwave sintering were found to lead to special microstructure and excellent thermal performance. The grain size of Zr 0.3 Ti 0.7 NiSn is ∼10 μm. The in-situ nanoscale pores and inclusions are about 300–500 nm. The highest ZT 0.60 for Zr 0.3 Ti 0.7 NiSn was achieved at 673 K.
Journal Title: Materials Letters
Year Published: 2017
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