Unsymmetrical thiosulfonates were synthesized from thiols and arenesulfonohydrazides by their electrolysis in undivided cell equipped with graphite anode and stainless steel cathode under high current density applying NH4I both as… Click to show full abstract
Unsymmetrical thiosulfonates were synthesized from thiols and arenesulfonohydrazides by their electrolysis in undivided cell equipped with graphite anode and stainless steel cathode under high current density applying NH4I both as a redox catalyst and a supporting electrolyte. In the course of the process, oxidative formation of S–S bond occurs with the loss of hydrazine moiety.
Keywords:
iodide mediated;
thiosulfonates arenesulfonohydrazides;
ammonium iodide;
electrosynthesis unsymmetrical;
mediated electrosynthesis;
unsymmetrical thiosulfonates
Journal Title: Mendeleev Communications
Year Published: 2019
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Journal Title: Mendeleev Communications
Year Published: 2019
Link to full text (if available)
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recommendations!