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Abstract Mesoporous silicalite-1 zeolites with large mesopore volume have been synthesized with the assisting of CO2 solvent. X-ray diffraction (XRD) patterns and scanning electron microscopy (SEM) images show that mesoporous… Click to show full abstract
Abstract Mesoporous silicalite-1 zeolites with large mesopore volume have been synthesized with the assisting of CO2 solvent. X-ray diffraction (XRD) patterns and scanning electron microscopy (SEM) images show that mesoporous silicalite-1 zeolites have good crystallinity. N2 sorption isotherm and transmission electron microscopy (TEM) images indicate the mesoporous silicalite-1 zeolites have mesopores. Catalytic tests for the vapor phase Beckmann rearrangement of cyclohexanone oxime show that mesoporous silicalite-1 zeolites have high conversion of cyclohexanone oxime and selectivity of e-caprolactam compared with conventional silicalite-1 zeolites.
Journal Title: Microporous and Mesoporous Materials
Year Published: 2020
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