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Abstract Two reversible polymorphic phase transformation of 2,3-butanedione, 2,3- bis[4,4′-bis(diethylamino)benzophenone hydrazone] (DEBH) have been identified in DSC experiment. Topotactic phase transformation of three polymorphs has been observed in variable temperature… Click to show full abstract
Abstract Two reversible polymorphic phase transformation of 2,3-butanedione, 2,3- bis[4,4′-bis(diethylamino)benzophenone hydrazone] (DEBH) have been identified in DSC experiment. Topotactic phase transformation of three polymorphs has been observed in variable temperature Single Crystal X-ray Diffraction experiment. The reversible phase transformation of bulk material has been confirmed by Powder X-ray diffraction study.
Keywords:
reversible polymorphic;
phase;
polymorphic phase;
temperature induced;
phase transformation
Journal Title: Journal of Molecular Structure
Year Published: 2018
Link to full text (if available)
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Journal Title: Journal of Molecular Structure
Year Published: 2018
Link to full text (if available)
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recommendations!