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Controlled synthesis of magnetic carbon nanoparticles via glycerol/ferrocene co-pyrolysis with magnetic induction

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Abstract We performed a controlled synthesis of magnetic carbon nanoparticles (M-CNPs) via co-pyrolysis of glycerol and ferrocene with magnetic induction. The morphology of the synthesized M-CNPs was confirmed by transmission… Click to show full abstract

Abstract We performed a controlled synthesis of magnetic carbon nanoparticles (M-CNPs) via co-pyrolysis of glycerol and ferrocene with magnetic induction. The morphology of the synthesized M-CNPs was confirmed by transmission electron microscopy, and thermogravimetric analysis was used to analyze the carbon and Fe contents. M-CNPs that responded to magnetic stimulation were also examined with an AC-magnetic susceptibility analyzer. Our investigations on the influence of synthesis temperature in the range 700–1000 °C suggested that for an initial glycerol to ferrocene weight ratio of 3:1 and a temperature of 800 °C gave the highest yield of M-CNPs. Comparing the synthesis with and without magnetic induction, the controlled synthesis under the influence of magnetic induction shows promise as a method for producing high quality M-CNPs in high yields.

Keywords: carbon; magnetic induction; glycerol ferrocene; controlled synthesis; induction

Journal Title: Particuology
Year Published: 2017

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