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Characterizing dispersion and long term stability of concentrated carbon nanotube aqueous suspensions for fabricating ductile cementitious composites

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Abstract This paper reports a systematic attempt of preparing concentrated aqueous suspensions (up to 0.3 wt.%) of different types of carbon nanotubes (CNTs) using Pluronic F-127 for developing ductile cementitious composites.… Click to show full abstract

Abstract This paper reports a systematic attempt of preparing concentrated aqueous suspensions (up to 0.3 wt.%) of different types of carbon nanotubes (CNTs) using Pluronic F-127 for developing ductile cementitious composites. Single-walled and multi-walled nanotubes, both pristine and functionalized, were dispersed in water using a short (1 h) and medium energy (80 W) ultrasonication process using pluronic at high concentrations (above critical micelle concentration, 1–5 wt.%) and also using sodium dodecylbenzene sulphonate (SDBS) for comparison purpose. The CNT suspensions were characterized for agglomerate area, particle size, zeta potential, extractability and long-term storage stability for a period over 4 years. The optimum suspensions were used to fabricate cementitious composites and their fracture behavior was characterized. Experimental results suggested that the optimum pluronic concentrations (1% for 0.1% CNT, 5% for 0.2% and 0.3% CNT, all in weight percent) provided highly homogeneous CNT dispersion with very low area of agglomerates. The best dispersion quality was obtained with f-SWCNT/pluronic system, which provided very low agglomerate area (

Keywords: aqueous suspensions; carbon; long term; dispersion; ductile cementitious; cementitious composites

Journal Title: Powder Technology
Year Published: 2017

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