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Local thermal conductivity measurements to determine the fraction of α-cristobalite in thermally grown oxides for aerospace applications

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Abstract Devitrification of the thermally grown oxide that forms in aerospace coatings used to protect ceramic matrix composites is a contributor to the mechanical failure of these coatings at high… Click to show full abstract

Abstract Devitrification of the thermally grown oxide that forms in aerospace coatings used to protect ceramic matrix composites is a contributor to the mechanical failure of these coatings at high operating temperatures. Current methods used to identify the formation of α-cristobalite are time consuming and difficult, due to the limited differences in properties as well as the size scale over which these phase contrasts occur. This study employs time-domain thermoreflectance to spatially profile the thermal conductivity of thermally aged samples, providing a practical method to understand the spatial distribution of α-cristobalite in partially- and fully-devitrified amorphous silica.

Keywords: thermally grown; conductivity measurements; thermal conductivity; local thermal; cristobalite

Journal Title: Scripta Materialia
Year Published: 2020

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