The sonochemical methods have been used as a straight forward method for the synthesis of various composite materials, including the transition metal dichalcogenide composites. In the present work, we report… Click to show full abstract
The sonochemical methods have been used as a straight forward method for the synthesis of various composite materials, including the transition metal dichalcogenide composites. In the present work, we report a simple sonochemical synthesis of CuS nanoplates decorated partially reduced graphene oxide (PrGO) nanocomposite for the first time. The PrGO-CuS nanocomposite was synthesized using bath-sonication (frequency: 37 kHz; power: 150 W) of graphene oxide (GO), and CuS precursors at 80 °C for 60 min. The physicochemical characterization (FESEM, XRD, FTIR, and Raman spectroscopy) results confirmed the successful formation of CuS nanoplates on PrGO nanosheets. The as-synthesized PrGO-CuS nanocomposite was further utilized for electroanalysis of dopamine neurotransmitter. The obtained electroanalytical results revealed that PrGO-CuS nanocomposite has superior electrochemical activity towards dopamine than those obtained for GO, CuS, and GO-CuS composite. The fabricated biosensor shows a lower limit of detection (0.022 µM) with a more comprehensive linear response range (0.1-155.1 µM) for the detection of dopamine. Moreover, the PrGO-CuS nanocomposite electrode was successfully used for the detection of dopamine in bovine serum albumin.
               
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