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Semi-Inverted Sample Preparation of Meteorites for High Resolution Analytical Electron Microscopy Using Correlative Raman Spectroscopy and Xe Plasma FIB

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Many materials have regions of interest (ROIs) that are beneath the surface. A focused ion beam (FIB) is used to remove material at the microscale in order to expose these… Click to show full abstract

Many materials have regions of interest (ROIs) that are beneath the surface. A focused ion beam (FIB) is used to remove material at the microscale in order to expose these subsurface ROIs for analysis [1]. When the ROI is to be analyzed using high-resolution analytical electron microscopy, the sample must be very thin (>100 nm) in order to allow transmission of electrons through the sample. The FIB is used not only for ROI extraction but also for thinning the sample to electron transparency [2]. However, when the ROI is more than a few microns beneath the surface and is surrounded by a mineralogically heterogeneous matrix, as is the case for most meteorites, it can be challenging to uniformly thin the ROI to >100 nm.

Keywords: microscopy; high resolution; spectroscopy; resolution analytical; analytical electron

Journal Title: Microscopy and Microanalysis
Year Published: 2019

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