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Thanks to a homemade dynamic vacuum system, fully crystallized VO2 (M) is successfully synthesized in a merged step of vanadyl ethylene glycolate (VEG) decomposition and crystallization of VO2 at high… Click to show full abstract
Thanks to a homemade dynamic vacuum system, fully crystallized VO2 (M) is successfully synthesized in a merged step of vanadyl ethylene glycolate (VEG) decomposition and crystallization of VO2 at high temperatures (>500 °C). During the whole process, vanadium valence (+4) is well maintained, and VEG microstructure plays an important role in the end-product size and shape. Finally, the suggested route appears well suitable for the mass production of VO2 nanoparticles.
Keywords:
micro nanoscale;
nanoscale vo2;
glycolate;
characterization micro;
decomposition;
synthesis characterization
Journal Title: Inorganic chemistry
Year Published: 2021
Link to full text (if available)
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Journal Title: Inorganic chemistry
Year Published: 2021
Link to full text (if available)
Share on Social Media: Sign Up to like & get
recommendations!