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Palladium-Catalyzed Domino Heck/Aryne Carbopalladation/C-H Functionalization: Synthesis of Heterocycle-Fused 9,10-Dihydrophenanthrenes.

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A novel palladium-catalyzed domino Heck/aryne carbopalladation/C-H functionalization reaction using in situ generated arynes has been developed in which three new C-C bonds and a carbon quaternary center are formed. This… Click to show full abstract

A novel palladium-catalyzed domino Heck/aryne carbopalladation/C-H functionalization reaction using in situ generated arynes has been developed in which three new C-C bonds and a carbon quaternary center are formed. This methodology affords moderate to excellent yields of heterocycle-fused 9,10-dihydrophenanthrenes.

Keywords: carbopalladation functionalization; domino heck; palladium catalyzed; heck aryne; catalyzed domino; aryne carbopalladation

Journal Title: Organic letters
Year Published: 2017

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