LAUSR

The current study demonstrates the synthesis of CuCo2S4 nanoparticles using a novel thermal decomposition approach. The CuCo2S4 nanoparticles were synthesized under various conditions by changing the source of sulfur and the solvent. The CuCo2S4 nanoparticles were characterized using an array of analytical techniques. Powder XRD results indicate the successful formation of CuCo2S4 nanoparticles. TEM results show agglomerated nanoparticles with close to spherical morphology and XPS measurements indicate the presence of Cu2+, Cu+, Co3+, Co2+, and S2- in the samples. The CuCo2S4 nanoparticles exhibit weak ferromagnetic and paramagnetic behaviour at 5 K and 300 K, respectively. The CuCo2S4 nanoparticles were explored for their enzyme mimetic activity using 3,3',5,5' tetramethylbenzidine (TMB) as a substrate. They exhibit better catalytic activity compared to that of a natural enzyme (horseradish peroxidase) and other metal sulfide nanoparticles reported in the literature.