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Many reduction reactions require the use of BH3, which is commercially available as complex in many different solvents. The determination of the content of BH3 in such solutions could be… Click to show full abstract
Many reduction reactions require the use of BH3, which is commercially available as complex in many different solvents. The determination of the content of BH3 in such solutions could be an important issue when the stoichiometry of the reaction is concerned. A fast, direct, and reproducible method to establish the content of BH3 in several solutions based on 11B NMR analysis is reported.
Keywords:
11b nmr;
practical 11b;
nmr evaluation;
bh3;
bh3 titer;
evaluation bh3
Journal Title: Synthesis
Year Published: 2017
Link to full text (if available)
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Journal Title: Synthesis
Year Published: 2017
Link to full text (if available)
Share on Social Media: Sign Up to like & get
recommendations!