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Preparation of TiAl15Si15 intermetallic alloy by mechanical alloying and the spark plasma sintering method

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ABSTRACT This work is devoted to the preparation of alloys based on intermetallic compounds in the Ti–Al–Si system by powder metallurgy using mechanical alloying and the spark plasma sintering (SPS)… Click to show full abstract

ABSTRACT This work is devoted to the preparation of alloys based on intermetallic compounds in the Ti–Al–Si system by powder metallurgy using mechanical alloying and the spark plasma sintering (SPS) method. The aim was to describe the formation of intermetallic phases during mechanical alloying of TiAl15Si15 (wt-%) alloy and to consolidate the powder prepared by optimised conditions. Phase composition, microstructure and hardness of compacted alloy were determined. Four hours of mechanical alloying is sufficient time for preparation of pure elements free material composed only of intermetallic phases. After consolidation, the TiAl15Si15 alloy has a homogeneous structure composed of silicide (Ti5Si3) in aluminide (TiAl) matrix. The hardness of the material reaches 865 ± 42 HV 5.

Keywords: plasma sintering; mechanical alloying; spark plasma; metallurgy; alloying spark; preparation

Journal Title: Powder Metallurgy
Year Published: 2019

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