In this article, Co0.40Zn0.40Cu0.20Fe2O4 (CoZCF) nanoparticles were synthesized using sol-gel method. The Field Emission Scanning Electron Microscopy (FESEM) micrographs delineate the proper encapsulation of the soft magnetic nanoparticles inside the… Click to show full abstract
In this article, Co0.40Zn0.40Cu0.20Fe2O4 (CoZCF) nanoparticles were synthesized using sol-gel method. The Field Emission Scanning Electron Microscopy (FESEM) micrographs delineate the proper encapsulation of the soft magnetic nanoparticles inside the matrix of multi-walled carbon nanotubes (MWCNTs) and ensuring proper fabrication of the CoZCF-MWCNT nanocomposites. The X-ray Diffraction (XRD) analysis and Raman spectroscopy confirms the presence of the multi-phase nature of CoZCF-MWCNT nanocomposites. The static magnetic development of the nanocomposites as a function of temperature and the shielding effectiveness behavior in X-band and Ku-band of microwave radiation have been studied herein. Different static magnetic quantities were extracted. The magnetic observation confirms the presence of ferrimagnetic state with magnetization of 48.4 and 44.8 emu gā1 respectively at room temperature (RT) in CoZCF-MWCNT nanocomposites. The variation of hysteresis loop area with the lowering of temperature depicts the transformation of CoZCF-MWCNT nanocomposites from superparamagnetic to ferromagnetic state. The shielding effectiveness study was conducted in the X- and Ku- bands of electromagnetic radiation and the observation shows a high value of total shielding effectiveness (SET) of ā¼ ā31.3 dB corresponding to 10.7 GHz. This is due to the high of attenuation of > 99.9% and wide bandwidth. This improved SET of CoZCF-MWCNT nanocomposites gives us completely new insights for the construction of microwave absorber/Radar Absorbing Materials (RAMs) that can contest against harmful electromagnetic pollution.
               
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