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In the present paper, the MnO2 films have been deposited on stainless steel support by potentiostatic mode of electrodeposition at different times. The x-ray diffraction, Fourier transform infrared spectroscopy along… Click to show full abstract
In the present paper, the MnO2 films have been deposited on stainless steel support by potentiostatic mode of electrodeposition at different times. The x-ray diffraction, Fourier transform infrared spectroscopy along with Energy-dispersive x-ray spectroscopy analysis confirmed formation of amorphous MnO2 coating. The surface analysis by field emission scanning electron microscope indicated development of fractures with increasing film thickness. The in situ measurement of stress to the substrate and MnO2 film thickness during deposition is performed by non-destructive double exposure digital holographic interferometry (DEDHI) technique. It was observed that the stress to the substrate decreases with increasing MnO2 film thickness. This study opens application of DEDHI for non-destructive measurement using simple mathematical interpretation.
Journal Title: Materials Research Express
Year Published: 2019
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