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Specific analysis of highly absorbing nanoporous powder by small-angle X-ray scattering

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The contributions of grain facet reflectivity and scattering from the bulk of a grain of highly absorbing material were calculated as a function of sample characteristics. To test these results,… Click to show full abstract

The contributions of grain facet reflectivity and scattering from the bulk of a grain of highly absorbing material were calculated as a function of sample characteristics. To test these results, the scattering intensity of a grain of microporous ThO2 was experimentally characterized by small-angle X-ray scattering using a synchrotron source. In addition, a new experimental method to probe the porous texture of nanoporous powders of highly absorbing compounds using a laboratory X-ray instrument has been proposed.

Keywords: highly absorbing; ray scattering; ray; angle ray; small angle

Journal Title: Journal of Applied Crystallography
Year Published: 2022

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