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Hierarchical synchrotron diffraction and imaging study of the calcium sulfate hemihydrate–gypsum transformation

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A combined approach of scanning 3D X-ray diffraction and phase contrast tomography has been used to study the hydration of calcium sulfate hemihydrate to form gypsum. This approach was found… Click to show full abstract

A combined approach of scanning 3D X-ray diffraction and phase contrast tomography has been used to study the hydration of calcium sulfate hemihydrate to form gypsum. This approach was found to be a powerful tool that permitted – for the first time – coupling of detailed crystallographic and morphological information on the hemihydrate–gypsum transition observed in situ.

Keywords: diffraction; calcium sulfate; hemihydrate; sulfate hemihydrate; hemihydrate gypsum; gypsum

Journal Title: Journal of Applied Crystallography
Year Published: 2023

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