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High-accuracy measurement of the X-ray absorption fine structure (XAFS) of zinc metal in a temperature series from 10 K to 150 K, including 298 K, simultaneously in transmission and fluorescence using the hybrid… Click to show full abstract
High-accuracy measurement of the X-ray absorption fine structure (XAFS) of zinc metal in a temperature series from 10 K to 150 K, including 298 K, simultaneously in transmission and fluorescence using the hybrid technique is presented: the first transition metal XAFS using the hybrid technique and at low temperatures; and the first (hybrid-like) experiment at the Australian Synchrotron. A methodology for relative measurements and a methodology for cryostat measurements, and an approach to normalization, calibration of transmission measurements for scattering and other systematics to reference room-temperature data and yield a defined uncertainty are presented.
Journal Title: Journal of Synchrotron Radiation
Year Published: 2023
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