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Nuclear Magnetic Resonance Measurements in High Flat-Top Pulsed Magnetic Field Up to 40 T at WHMFC

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The nuclear magnetic resonance (NMR) technique benefits from the high magnetic field not only due to the field-enhanced measurement sensitivity and resolution, but also because it is a powerful tool… Click to show full abstract

The nuclear magnetic resonance (NMR) technique benefits from the high magnetic field not only due to the field-enhanced measurement sensitivity and resolution, but also because it is a powerful tool to investigate field-induced physics in modern material science. In this study, we successfully performed NMR measurements in the high flat-top pulsed magnetic field (FTPMF) up to 40 T. A two-stage corrected FTPMF with fluctuation of less than 10 mT and duration of longer than 9 ms was established. Besides, a Giga-Hz NMR spectrometer and a sample probe suitable for the pulsed-field condition were developed. Both free-induction-decay (FID) and spin-echo (SE) sequences were exploited for the measurements. The derived 93Nb NMR results show that the stability and homogeneity of the FTPMF reach an order of $10^{2}$ ppm/10 ms and $10^{2}$ ppm/10 mm3, respectively, which is approaching a degree of maturity for some researches on condensed matter physics.

Keywords: magnetic resonance; nuclear magnetic; high flat; magnetic field; field; measurements high

Journal Title: IEEE Transactions on Instrumentation and Measurement
Year Published: 2022

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