The synthesis of iridium powder in a molten NaCl–KCl medium at 700°C is carried out for the first time. The influence of the ratio of the cathode to the anode… Click to show full abstract
The synthesis of iridium powder in a molten NaCl–KCl medium at 700°C is carried out for the first time. The influence of the ratio of the cathode to the anode current density (ic/ia) on the structure and the morphology of the iridium powder is investigated. Single-phase and polycrystalline iridium powders with a specific surface of 16.8 m2/g are produced. The phase composition and the surface texture of the deposits are studied. The specific surface and the particle size of iridium powders as functions of the ratio ic/ia are analyzed.
               
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