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One-pot synthesis of azo compounds in the absence of acidic or alkaline additives

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A one-pot method for the synthesis of azo compounds by the reaction of β-naphthol with aryl amines using t-BuONO as the nitrosonium source in DCM at room temperature was developed.… Click to show full abstract

A one-pot method for the synthesis of azo compounds by the reaction of β-naphthol with aryl amines using t-BuONO as the nitrosonium source in DCM at room temperature was developed. This method features mild reaction conditions, a simple experimental procedure, and is free of acidic or alkaline additives.

Keywords: azo compounds; synthesis azo; alkaline additives; one pot; acidic alkaline

Journal Title: Journal of Chemical Research
Year Published: 2020

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