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Microwave irradiation was applied to a sterically demanding ring-closing metathesis catalyzed by a second-generation Grubbs catalyst. Under strict temperature control, reaction acceleration by microwave irradiation was observed. The observed acceleration… Click to show full abstract
Microwave irradiation was applied to a sterically demanding ring-closing metathesis catalyzed by a second-generation Grubbs catalyst. Under strict temperature control, reaction acceleration by microwave irradiation was observed. The observed acceleration effect was estimated to be equivalent to a rising temperature of 2.5–5 °C range under conventional heating conditions.
Keywords:
enhancement ring;
ring closing;
closing metathesis;
microwave enhancement;
metathesis macrocyclic
Journal Title: Chemistry Letters
Year Published: 2017
Link to full text (if available)
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Journal Title: Chemistry Letters
Year Published: 2017
Link to full text (if available)
Share on Social Media: Sign Up to like & get
recommendations!