Applications of high‐resolution magic angle spinning MRS in biomedical studies I—cell line and animal models
Sign Up to like & getrecommendations! Published in 2017 at "NMR in Biomedicine"
DOI: 10.1002/nbm.3700
Abstract: High‐resolution magic angle spinning (HRMAS) MRS allows for direct measurements of non‐liquid tissue and cell specimens to present valuable insights into the cellular metabolisms of physiological and pathological processes. HRMAS produces high‐resolution spectra comparable to… read more here.
Keywords: high resolution; magic angle; angle spinning; resolution magic ... See more keywords
Applications of high‐resolution magic angle spinning MRS in biomedical studies II—Human diseases
Sign Up to like & getrecommendations! Published in 2017 at "NMR in Biomedicine"
DOI: 10.1002/nbm.3784
Abstract: High‐resolution magic angle spinning (HRMAS) MRS is a powerful method for gaining insight into the physiological and pathological processes of cellular metabolism. Given its ability to obtain high‐resolution spectra of non‐liquid biological samples, while preserving… read more here.
Keywords: resolution; high resolution; biomedical studies; magic angle ... See more keywords
Determination of methyl order parameters using solid state NMR under off magic angle spinning.
Sign Up to like & getrecommendations! Published in 2019 at "Journal of biomolecular NMR"
DOI: 10.1007/s10858-019-00253-5
Abstract: Quantification of dipolar couplings in biological solids is important for the understanding of dynamic processes. Under Magic Angle Spinning (MAS), order parameters are normally obtained by recoupling of anisotropic interactions involving the application of radio… read more here.
Keywords: order; methyl order; order parameters; magic angle ... See more keywords
A New Method of Assessing Lipid Mixtures by 31P Magic-Angle Spinning NMR.
Sign Up to like & getrecommendations! Published in 2018 at "Biophysical journal"
DOI: 10.1016/j.bpj.2018.01.025
Abstract: A variety of lipids that differ by their chains and headgroups are found in biomembranes. In addition to studying the overall membrane phase, determination of the structure, dynamics, and headgroup conformation of individual lipids in… read more here.
Keywords: method assessing; chemical shift; new method; magic angle ... See more keywords
High-resolution magic angle spinning nuclear magnetic resonance (HR-MAS NMR) as a tool in the determination of biomarkers of Passiflora-based herbal medicines.
Sign Up to like & getrecommendations! Published in 2020 at "Fitoterapia"
DOI: 10.1016/j.fitote.2020.104500
Abstract: High-resolution magic-angle spinning nuclear magnetic resonance spectroscopy (HR-MAS NMR) for the identification of the metabolic profile of plants under conditions very close to that in which the compounds are present in the matrix, the herbal… read more here.
Keywords: high resolution; mas nmr; herbal medicines; magic angle ... See more keywords
Metabolic profiling of apples from different production systems before and after controlled atmosphere (CA) storage studied by 1H high resolution-magic angle spinning (HR-MAS) NMR.
Sign Up to like & getrecommendations! Published in 2017 at "Food chemistry"
DOI: 10.1016/j.foodchem.2017.04.089
Abstract: Determination of metabolic alterations in apples induced by such processes as different crop protection strategies or storage, are of interest to assess correlations with fruit quality or fruit disorders. Preliminary results proposed the metabolic discrimination… read more here.
Keywords: high resolution; production; spinning mas; magic angle ... See more keywords
1H magic-angle spinning NMR evolves as a powerful new tool for membrane proteins.
Sign Up to like & getrecommendations! Published in 2018 at "Journal of magnetic resonance"
DOI: 10.1016/j.jmr.2017.11.014
Abstract: Building on a decade of continuous advances of the community, the recent development of very fast (60 kHz and above) magic-angle spinning (MAS) probes has revolutionised the field of solid-state NMR. This new spinning regime reduces… read more here.
Keywords: membrane proteins; nmr evolves; spinning nmr; magic angle ... See more keywords
A versatile custom cryostat for dynamic nuclear polarization supports multiple cryogenic magic angle spinning transmission line probes.
Sign Up to like & getrecommendations! Published in 2018 at "Journal of magnetic resonance"
DOI: 10.1016/j.jmr.2018.10.002
Abstract: Dynamic nuclear polarization (DNP) with cryogenic magic angle spinning (MAS) provides significant improvements in NMR sensitivity, yet presents unique technical challenges. Here we describe a custom cryostat and suite of NMR probes capable of manipulating… read more here.
Keywords: cryogenic magic; cryostat; nuclear polarization; magic angle ... See more keywords
29Si, 27Al, 31P and 11B magic angle spinning nuclear magnetic resonance study of the structural evolutions induced by the use of phosphor- and boron–based additives in geopolymer mixtures
Sign Up to like & getrecommendations! Published in 2019 at "Journal of Non-Crystalline Solids"
DOI: 10.1016/j.jnoncrysol.2019.119541
Abstract: Abstract This study aims to develop a geopolymer binder, which requires a control of the reactive mixture setting time, viscosity and pH value. A previous study underlines the possibility of controlling the setting time, viscosity… read more here.
Keywords: boron based; magic angle; angle spinning; study ... See more keywords
Fast 19F Magic Angle Spinning NMR Crystallography for Structural Characterization of Fluorine-Containing Pharmaceutical Compounds.
Sign Up to like & getrecommendations! Published in 2021 at "Analytical chemistry"
DOI: 10.1021/acs.analchem.1c00784
Abstract: Fluorine-containing compounds comprise 20 to 30 percent of all commercial drugs, and the proportion of fluorinated pharmaceuticals is rapidly growing. While magic angle spinning (MAS) NMR spectroscopy is a popular technique for analysis of solid… read more here.
Keywords: structural characterization; pharmaceutical compounds; fluorine; magic angle ... See more keywords
Dynamic Sorting of Mobile and Rigid Molecules in Biomembranes by Magic-Angle Spinning 13C NMR.
Sign Up to like & getrecommendations! Published in 2023 at "Analytical chemistry"
DOI: 10.1021/acs.analchem.2c04185
Abstract: Understanding the membrane dynamics of complex systems is essential to follow their function. As molecules in membranes can be in a rigid or mobile state depending on external (temperature, pressure) or internal (pH, domains, etc.)… read more here.
Keywords: angle spinning; sorting mobile; magic angle; mobile rigid ... See more keywords