Synthesis and Structural Characterisation of Lithium, Zinc, and Aluminium Pyrazolate Complexes
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DOI: 10.1071/ch19417
Abstract: The reaction of nBuLi with 3,5-dimethylpyrazole (Me2pzH) in Et2O or tmeda/hexane (tmeda = N,N,N′,N′-tetramethylethane-1,2-diamine) and with 3,5-dimethyl-4-nitropyrazolate (Me2pzHNO2) in THF results in the formation of three structurally diverse lithium pyrazolates: namely an Et2O-solvated tetrameric complex [Li4(Me2pz)4(OEt2)4], bridged… read more here.
Keywords: zinc; synthesis structural; thf; structural characterisation ... See more keywords