Synthesis, characterization and X-ray crystal structure of Tp*WII{(R)-(+)-NHCH(Me)Ph}(CO)2
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DOI: 10.1016/j.ica.2020.120016
Abstract: Abstract Reaction of Tp*WIII(CO)2 [Tp* = hydrotris(3,5-dimethylpyrazol-1-yl)borate] with (R)-(+)-α-methylbenzylamine [(R)-(+)-LH2] in dichloromethane yields blue, diamagnetic Tp*WII{(R)-(+)-LH}(CO)2, which has been characterised by microanalysis, mass spectrometry, infrared, 1H NMR, 13C{1H} NMR and electronic spectroscopies, and X-ray crystallography.… read more here.
Keywords: wii; synthesis characterization; characterization ray; crystal structure ... See more keywords
Synthesis, characterization, X-ray crystallography and stability in aqueous medium of trans -[Ru(CO)(NH 3 ) 4 P(OH) 3 ] 2+
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DOI: 10.1016/j.poly.2016.12.019
Abstract: Abstract Here, we report the synthesis, characterization, crystal data and DFT calculation of a new water-soluble ruthenium(II) carbonyl complex. The trans-[Ru(CO)(NH3)4P(O)(OH)2]Cl is a robust complex in aqueous media. The pKa of 3.3 for the phosphorous… read more here.
Keywords: trans nh3; crystallography stability; characterization ray; ray crystallography ... See more keywords
Synthesis, Characterization and X-Ray Crystal Structures of Schiff Base Zinc(II) Complexes with Antibacterial Activity.
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DOI: 10.17344/acsi.2024.8928
Abstract: Two mononuclear zinc(II) complexes [ZnCl2(HL)] (1) and [ZnBr2(HL)] (2), and a polymeric zinc(II) complex [Zn(dca)L] (3), where HL is the zwitterionic form of the Schiff base 2,4-difluoro-6-(((2-pyrrolidin-1-yl)ethylimino)methyl)phenol (HL), L is the monoanionic form of HL,… read more here.
Keywords: zinc complexes; characterization ray; schiff base; zinc ... See more keywords
Synthesis, Characterization and X-Ray Crystal Structures of Aroylhydrazones Derived from 2-Chlorobenzaldehyde with Various Benzohydrazides
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DOI: 10.17344/acsi.2024.8967
Abstract: Reaction of 2-chlorobenzaldehyde with 3-trifluoromethylbenzohydrazide, 3,5-dimethoxybenzohydrazide, 4-trifluoromethylbenzohydrazide and 2-bromobenzohydrazide, respectively, in methanol afforded four new aroylhydrazones. The newly synthesized compounds were characterized by means of elemental analysis, IR and 1H NMR spectroscopy, and their structures… read more here.
Keywords: characterization ray; aroylhydrazones derived; ray crystal; synthesis characterization ... See more keywords