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Published in 2018 at "Synlett"
DOI: 10.1055/s-0037-1610334
Abstract: In the functionalization of salicylaldehyde to give 5-(chloromethyl)salicylaldehyde, two byproducts [5-(hydroxymethyl)salicylaldehyde and 5,5′-methylenebis(salicylaldehyde)] were also isolated. Detailed characterizations and structural analyses of all three products by single-crystal X-ray diffraction, multinuclear NMR spectroscopy, high-resolution mass spectrometry,…
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Keywords:
products chloromethylation;
structural identification;
chloromethylation salicylaldehyde;
spectroscopy ... See more keywords