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Published in 2020 at "Organic letters"
DOI: 10.1021/acs.orglett.0c03210
Abstract: Herein, we present a nickel-catalyzed three-component reductive alkylacylation of electron-deficient activated alkenes with tertiary alkyl bromides and acid anhydrides. This method enables the efficient preparation of a variety of ketones with broad substrate scope and…
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Keywords:
alkylacylation electron;
catalyzed three;
component reductive;
three component ... See more keywords
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Published in 2022 at "Chemical communications"
DOI: 10.1039/d2cc05330f
Abstract: A three-component reductive coupling reaction of aldehydes, amines and cyanopyridines under electrochemical conditions has been developed. The in situ generated imine and cyanopyridine simultaneously undergo single-electron reduction at the cathode, and afford diarylmethylamines through radical…
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Keywords:
electricity driven;
coupling reaction;
reductive coupling;
component reductive ... See more keywords
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Published in 2023 at "Chemical Science"
DOI: 10.1039/d2sc06303d
Abstract: A three-component reductive cross-coupling of aryl halides, aldehydes, and alkenes by nickel/photoredox dual catalysis is disclosed. The key to success for this tandem transformation is to identify α-silylamine as a unique organic reductant, which releases…
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Keywords:
conjugate addition;
component reductive;
dual catalysis;
photoredox dual ... See more keywords