Compressibility of hingganite-(Y): high-pressure single crystal X-ray diffraction study
Sign Up to like & getrecommendations! Published in 2020 at "Physics and Chemistry of Minerals"
DOI: 10.1007/s00269-020-01090-x
Abstract: Behaviour of hingganite-(Y), Y2□Be2Si2O8(OH)2, on compression to 47 GPa has been studied by synchrotron-based in situ high-pressure single-crystal X-ray diffraction at room temperature in a diamond anvil cell. In the studied pressure range no obvious… read more here.
Keywords: ray diffraction; single crystal; crystal ray; high pressure ... See more keywords
Unexpected identification of a bupivacaine analog from smuggling by using single-crystal X-ray diffraction analysis: N-(2,6-dimethylphenyl)-1-phenethylpiperidine-2-carboxamide.
Sign Up to like & getrecommendations! Published in 2021 at "Forensic science international"
DOI: 10.1016/j.forsciint.2021.110917
Abstract: The identification of new psychoactive substances (NPSs) is essential against drug abuse, especially for "new" drugs that are not regulated by international drug conventions. A suspicious powder seized by the officers of Taipei Customs Administration… read more here.
Keywords: single crystal; dimethylphenyl phenethylpiperidine; crystal ray; identification ... See more keywords
Single-crystal x-ray diffraction and impedance spectroscopy investigations of the RbxCs1-xH2PO4 (0≤x≤1) proton conductor series
Sign Up to like & getrecommendations! Published in 2018 at "Journal of Physics and Chemistry of Solids"
DOI: 10.1016/j.jpcs.2018.03.011
Abstract: Abstract We have used single-crystal x-ray diffraction to investigate the structural modifications induced by Rb-doping of the superprotonic conductor CsH 2 PO 4 . We found that the monoclinic P 2 1 / m CsH… read more here.
Keywords: temperature; ray diffraction; single crystal; crystal ray ... See more keywords
Synthesis, characterization and single crystal X-ray analysis of Zn(II) phenanthridine complexes
Sign Up to like & getrecommendations! Published in 2019 at "Journal of Molecular Structure"
DOI: 10.1016/j.molstruc.2019.01.002
Abstract: Abstract Reaction of the phenanthridine ligand (phend) with ZnBr2 in DMSO/MeOH or MeOH yielded the complexes ZnBr2(phend)(DMSO) (1) and ZnBr2(phend)2 (2) respectively. These complexes were characterized by single crystal X-ray diffraction, IR spectroscopy and elemental… read more here.
Keywords: crystal; synthesis characterization; crystal ray; single crystal ... See more keywords
Syntheses, single crystal X-ray structure, Hirshfeld surface analyses, DFT computations and Monte Carlo simulations of New Eugenol derivatives bearing 1,2,3-triazole moiety
Sign Up to like & getrecommendations! Published in 2021 at "Journal of Molecular Structure"
DOI: 10.1016/j.molstruc.2021.130189
Abstract: Abstract A novel series of 1,2,3-triazole derivatives containing the eugenol ring (3 and 4) were synthesized in good yields (78 and 82%, respectively) by click chemistry method [Copper-Catalyzed Azide-Alkyne Cycloaddition (CuAAC)]. We report here the… read more here.
Keywords: surface analyses; monte carlo; crystal ray; single crystal ... See more keywords
Syntheses and single crystal X-ray diffraction studies of hydroxynicotinic acid based complexes involving supramolecular interactions
Sign Up to like & getrecommendations! Published in 2017 at "Polyhedron"
DOI: 10.1016/j.poly.2017.05.041
Abstract: Abstract Aqua-bridged coordination polymers of Cu(II) and Cd(II) and a mononuclear complex of Cu(II) were solvothermally synthesized with hydroxy-decorated ligands such as 2-hydroxynicotinic acid (2-OHNAH) and 6-hydroxynicotinic acid (6-OHNAH) in aqueous-nonaqueous mixed media. All these… read more here.
Keywords: supramolecular interactions; single crystal; crystal ray; syntheses single ... See more keywords
Significance of an Environmental Gas Cell to Obtain a Fully Dehydrated Form and CO2-Pressurized Structure of a Metal-Organic Framework Using In Situ Single-Crystal X-ray Diffraction at 298 K.
Sign Up to like & getrecommendations! Published in 2022 at "Inorganic chemistry"
DOI: 10.1021/acs.inorgchem.1c02933.s002
Abstract: The single-crystal X-ray diffraction method was employed to characterize a rigid hydrated metal-organic framework (MOF), [Co2(MA)(INA)·2H2O]n, that displays an affinity toward water molecules under ambient conditions after dehydration. The fully dehydrated form was obtained using… read more here.
Keywords: single crystal; organic framework; ray diffraction; metal organic ... See more keywords
Strontium Nitridoborate Hydride Sr2BN2H Verified by Single-Crystal X-ray and Neutron Powder Diffraction.
Sign Up to like & getrecommendations! Published in 2022 at "Inorganic chemistry"
DOI: 10.1021/acs.inorgchem.2c01688
Abstract: Combining different anions in one material allows tuning of its structural, magnetic, and electronic properties. We hereby present the mixed anion compound Sr2BN2H, expanding the less-known class of nitridoborate hydrides. Solid-state reaction of Sr2N, BN,… read more here.
Keywords: sr2bn2h; single crystal; neutron powder; powder ... See more keywords
Determination of d-Orbital Populations in a Cobalt(II) Single-Molecule Magnet Using Single-Crystal X-ray Diffraction.
Sign Up to like & getrecommendations! Published in 2018 at "Inorganic chemistry"
DOI: 10.1021/acs.inorgchem.8b00513
Abstract: The tetrahedral cobalt(II) compound (Ph4P)2[Co(SPh)4] was the first mononuclear transition-metal complex shown to exhibit slow relaxation of the magnetization in zero external magnetic field. Because the relative populations of the d orbitals play a vital… read more here.
Keywords: crystal ray; orbital populations; single crystal; ray diffraction ... See more keywords
Structure Reassignment of Echinosulfone A and the Echinosulfonic Acids A-D Supported by Single-Crystal X-ray Diffraction and Density Functional Theory Analysis.
Sign Up to like & getrecommendations! Published in 2020 at "Journal of natural products"
DOI: 10.1021/acs.jnatprod.9b00902
Abstract: Two previously reported bis-indole alkaloids, echinosulfone A and echinosulfonic acid B, have been isolated for the first time from a Western Australian marine sponge, Crella sp. (order: Poecilosclerida, family: Crellidae). Single-crystal X-ray diffraction of a… read more here.
Keywords: structure reassignment; ray diffraction; echinosulfone echinosulfonic; single crystal ... See more keywords
Reassigning the Pressure-Induced Phase Transitions of Methylammonium Lead Bromide Perovskite.
Sign Up to like & getrecommendations! Published in 2022 at "Journal of the American Chemical Society"
DOI: 10.1021/jacs.2c09457
Abstract: The high-pressure crystal structure evolution of CH3NH3PbBr3 (MAPbBr3) perovskite has been investigated by single-crystal X-ray diffraction and synchrotron-based powder X-ray diffraction. Single-crystal X-ray diffraction reveals that the crystal structure of MAPbBr3 undergoes two phase transitions… read more here.
Keywords: single crystal; pressure; ray diffraction; crystal ray ... See more keywords