Ligand-Enabled Sequential C(sp3)-H and C(sp2)-H Diolefination Reaction via Palladium Catalyst.
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DOI: 10.1021/acs.orglett.2c02502
Abstract: Palladium-catalyzed sequential C(sp3)-H and C(sp2)-H bond diolefination reaction of o-toluidine has been realized for the first time using acetyl-protected aminoethyl phenyl thioether ligands. This novel reaction allows for preparation of the conjugated diene structure via… read more here.
Keywords: diolefination reaction; sequential sp3; diolefination; reaction ... See more keywords