An in-situ x-ray diffraction and infrared spectroscopic study of the dehydration of AlPO4-54
Sign Up to like & getrecommendations! Published in 2020 at "Solid State Sciences"
DOI: 10.1016/j.solidstatesciences.2020.106378
Abstract: Abstract The dehydration of the large pore aluminophosphate AlPO4-54•xH2O was studied in situ as a function of vacuum pressure at room temperature by infrared spectroscopy and x-ray diffraction. On polycrystalline samples, under primary vacuum, the… read more here.
Keywords: vacuum; dehydration; fully dehydrated; ray diffraction ... See more keywords
Significance of an Environmental Gas Cell to Obtain a Fully Dehydrated Form and CO2-Pressurized Structure of a Metal-Organic Framework Using In Situ Single-Crystal X-ray Diffraction at 298 K.
Sign Up to like & getrecommendations! Published in 2022 at "Inorganic chemistry"
DOI: 10.1021/acs.inorgchem.1c02933.s002
Abstract: The single-crystal X-ray diffraction method was employed to characterize a rigid hydrated metal-organic framework (MOF), [Co2(MA)(INA)·2H2O]n, that displays an affinity toward water molecules under ambient conditions after dehydration. The fully dehydrated form was obtained using… read more here.
Keywords: single crystal; organic framework; ray diffraction; metal organic ... See more keywords