Articles with "headspace gas" as a keyword



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Comprehensive headspace gas chromatographic analysis of denaturants in denatured ethanol.

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Published in 2017 at "Journal of separation science"

DOI: 10.1002/jssc.201700468

Abstract: To discourage consumption, ethanol is often denatured using both volatile (e.g., methyl ethyl ketone and isopropanol) and nonvolatile (e.g., denatonium benzoate) chemical substances. As a result, the analysis of denatured ethanol samples is usually performed… read more here.

Keywords: denatured ethanol; chromatography; analysis; denaturants denatured ... See more keywords

Determination of 3-chloro-1,2-propanediol in polyamideamine epichlorohydrin resin solution by reaction-based headspace gas chromatography.

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Published in 2018 at "Journal of separation science"

DOI: 10.1002/jssc.201701079

Abstract: We report on a headspace gas chromatographic method for determining the content of 3-chloro-1,2-propanediol in polyamideamine epichlorohydrin resin solution. It was based on quantitatively converting 3-chloro-1,2-propanediol to formaldehyde by periodate oxidation in a closed headspace… read more here.

Keywords: chloro; polyamideamine epichlorohydrin; chloro propanediol; headspace gas ... See more keywords
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A Novel Method for Detection of Fusel Oil in Wine by the Use of Headspace Gas Chromatography

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Published in 2017 at "Food Analytical Methods"

DOI: 10.1007/s12161-017-0884-4

Abstract: Fusel oils (FOs) are higher alcohols (including propanol, isobutanol, isoamylol, and active amyl alcohol), which affect the aroma profiles and flavor profiles of wine. A novel method for determination of FOs in lychee wine was… read more here.

Keywords: gas chromatography; novel method; wine; method ... See more keywords
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Analysis of flavor formation during production of Dezhou braised chicken using headspace-gas chromatography-ion mobility spec-trometry (HS-GC-IMS).

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Published in 2021 at "Food chemistry"

DOI: 10.1016/j.foodchem.2021.130989

Abstract: In order to help the poultry industry to generate higher quality products, the headspace-gas chromatography-ion mobility spectrometry (HS-GC-IMS) technique was used to identify volatile substances formed during the processing of Dezhou braised chicken (DBC). A… read more here.

Keywords: gas chromatography; chromatography ion; flavor; ion mobility ... See more keywords
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Rapid determination of formic and acetic acids in biomass hydrolysate by headspace gas chromatography

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Published in 2017 at "Journal of Industrial and Engineering Chemistry"

DOI: 10.1016/j.jiec.2016.11.044

Abstract: A headspace gas chromatography (HS-GC) method is developed for determination of formic acid (FA) and acetic acid (AA) in biomass hydrolysate. The method is based on the “in-vial” derivatization reaction of alcohols and acids. NaHSO4/ethanol… read more here.

Keywords: gas chromatography; biomass; biomass hydrolysate; determination formic ... See more keywords
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Characterization of volatiles in Allium tenuissimum L. flower by headspace-gas chromatography-olfactometry-mass spectrometry, odor activity values, and the omission and recombination experiments

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Published in 2021 at "Lwt - Food Science and Technology"

DOI: 10.1016/j.lwt.2021.112144

Abstract: Abstract Volatiles in four Allium tenuissimum flower samples were detected and characterized by headspace-gas chromatography-olfactometry-mass spectrometry, and odor activity values. The key aroma compounds were determined by combining the sensory analysis with the omission and… read more here.

Keywords: allium tenuissimum; chromatography olfactometry; gas chromatography; tenuissimum flower ... See more keywords
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Assay of ethanol and congener alcohols in serum and beverages by headspace gas chromatography/mass spectrometry

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Published in 2021 at "MethodsX"

DOI: 10.1016/j.mex.2021.101563

Abstract: The analysis of ethanol and of its congeners in blood plays an important role in forensic cases, especially when allegations are made that alcohol has been consumed after an accident. In alcoholic beverages, congener alcohols… read more here.

Keywords: gas chromatography; congener alcohols; chromatography mass; headspace gas ... See more keywords
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Determination of hexavalent chromium in solid waste hypochlorite treated leachates by headspace gas chromatography

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Published in 2020 at "Microchemical Journal"

DOI: 10.1016/j.microc.2019.104494

Abstract: Abstract This article reported a new headspace gas chromatography (HS-GC) for the determination of hexavalent chromium Cr(VI) in solid waste hypochlorite treated leachates. The method was based on the reaction between Cr(VI) and an excess… read more here.

Keywords: gas chromatography; chromium solid; determination hexavalent; hypochlorite ... See more keywords
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Volatile-Based Prediction of Sauvignon Blanc Quality Gradings with Static Headspace-Gas Chromatography-Ion Mobility Spectrometry (SHS-GC-IMS) and Interpretable Machine Learning Techniques.

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Published in 2021 at "Journal of agricultural and food chemistry"

DOI: 10.1021/acs.jafc.0c07899

Abstract: The analytical scope of static headspace-gas chromatography-ion mobility spectrometry (SHS-GC-IMS) was applied to wine aroma analysis for the first time. The method parameters were first fine-tuned to achieve optimal analytical results, before the method stability… read more here.

Keywords: quality; chemistry; headspace gas; shs ims ... See more keywords
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Development of a Sensitive Headspace Gas Chromatography–Mass Spectrometry Method for the Simultaneous Determination of Nitrosamines in Losartan Active Pharmaceutical Ingredients

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Published in 2021 at "ACS Omega"

DOI: 10.1021/acsomega.1c00982

Abstract: Nitrosamine impurities in angiotensin II receptor antagonists (sartans) containing a tetrazole group represent an urgent concern for active pharmaceutical ingredient (API) manufacturers and global regulators. Regarding safety, API manufacturers must develop methods to monitor the… read more here.

Keywords: active pharmaceutical; nitrosamines losartan; method; mass ... See more keywords
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Technical note: Evaluation of sampling methods for methane concentration from in vitro fermentation.

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Published in 2022 at "Journal of animal science"

DOI: 10.1093/jas/skac259

Abstract: The objectives of this multi-part study were: 1.) to assess the efficacy of sampling methods of methane concentration ([CH4]) of headspace gas produced during in vitro gas production (IVGP) fermentation, 2.) to verify if headspace… read more here.

Keywords: gas; ch4; headspace gas; ivgp ... See more keywords