Mechanochemical Synthesis of N-Aryl Amides from O-Protected Hydroxamic Acids.
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DOI: 10.1002/cplu.202000451
Abstract: Two robust and efficient mechanochemical protocols for the synthesis of an array of N-arylamides have been developed. This was achieved by a C-N cross-coupling between O-pivaloyl hydroxamic acids and aryl iodides or aryl boronic acids,… read more here.
Keywords: hydroxamic acids; amides protected; mechanochemical synthesis; aryl amides ... See more keywords
Mechanistic Insights into a Sustainable Mechanochemical Synthesis of Ettringite
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DOI: 10.1002/open.201900215
Abstract: Abstract Mechanochemistry offers an environmentally benign and facile synthesis method for a variety of cement paste constituents. In addition, these methods can be used to selectively tune the properties of cement components. The mineral ettringite… read more here.
Keywords: insights sustainable; synthesis; mechanochemical synthesis; sustainable mechanochemical ... See more keywords
Rapid mechanochemical synthesis of nanostructured mohite Cu2SnS3 (CTS)
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DOI: 10.1007/s10853-018-2499-6
Abstract: Rapid solvent-free mechanochemical synthesis of CTS nanocrystals from elemental precursors is reported herein. The process is completed in 15 min, proceeding through immediate formation of CuS in a self-sustaining manner and its subsequent reaction with Sn… read more here.
Keywords: rapid mechanochemical; mohite cu2sns3; nanostructured mohite; mechanochemical synthesis ... See more keywords
Mechanochemical Synthesis of Hafnium Carbide using Amorphous Carbon from Plant Materials
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DOI: 10.1007/s11015-020-00934-9
Abstract: The paper presents the results of studying mechanochemical synthesis of hafnium carbide in the process of vibration treatment of the mixture of powders of hafnium and amorphous carbon obtained by pyrolytic processing of plant materials.… read more here.
Keywords: hafnium carbide; mechanochemical synthesis; plant materials;
Mechanochemical synthesis of platinum(IV) complexes with N-heterocyclic carbenes
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DOI: 10.1007/s11172-018-2321-2
Abstract: A new method for the synthesis of complexes PtIV(NHC)X4L (NHC is N-heterocyclic carbene of imidazole or benzimidazole series; X = Cl, Br; L is N-coordinated pyridine or NHC) based on mechanochemical oxidation of complexes PtII(NHC)X2L… read more here.
Keywords: platinum complexes; heterocyclic carbenes; mechanochemical synthesis; complexes heterocyclic ... See more keywords
On the features of mechanochemical synthesis of Y-Cu equiatomic powder mixture
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DOI: 10.1016/j.apt.2018.01.029
Abstract: Abstract Structural features of nanocomposite YCu powder material obtained by mechanical alloying of the equiatomic Y-Cu elemental powder mixture in a high-energy ball mill have been characterized by X-ray diffraction, and scanning electron microscopy. It… read more here.
Keywords: synthesis equiatomic; powder mixture; powder; mechanochemical synthesis ... See more keywords
Mechanochemical synthesis of BiSI and Bi19S27I3 semiconductor materials
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DOI: 10.1016/j.apt.2019.06.007
Abstract: Abstract With regard to the intensive investigations of bismuth oxyhalides as promising photocatalysts, much expectation may be put on the corresponding chalcohalides but little is known due to difficulty in the synthesis. In this report,… read more here.
Keywords: synthesis; mechanochemical synthesis; semiconductor materials; bi19s27i3 semiconductor ... See more keywords
Cobalt ferrite magnetic nanoparticles as highly efficient catalyst for the mechanochemical synthesis of 2-aryl benzimidazoles
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DOI: 10.1016/j.catcom.2021.106349
Abstract: Abstract A highly efficient magnetically separable nano cobalt ferrite catalyst was synthesized via the sol-gel auto combustion method, characterized by powder XRD, SEM, TEM, UV–Visible, FT-IR, magnetic study, and BET isotherm analysis. The synthesized material… read more here.
Keywords: synthesis; catalyst; cobalt ferrite; synthesis aryl ... See more keywords
Reaction mechanism in mechanochemical synthesis of Cu2-xSe
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DOI: 10.1016/j.ceramint.2018.08.331
Abstract: Abstract This paper investigates the reaction mechanism in mechanochemical synthesis of Cu 2-x Se by vibrational milling of (Cu+Se) powder mixture. The effects of milling time, milling mode, ball-to-powder weight ratio (BPWR), and Cu/Se molar… read more here.
Keywords: mechanochemical synthesis; reaction mechanism; mechanism mechanochemical; synthesis ... See more keywords
Mechanochemical synthesis of SrFe12O19 from recycled mill scale: Effect of synthesis time on phase formation and magnetic properties
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DOI: 10.1016/j.jallcom.2021.159787
Abstract: Abstract In the present study, the strontium hexaferrite (SrFe12O19) has been successfully produced from recycled mill scale and strontium carbonate (SrCO3) powders with stoichiometric ratio (SrCO3/Fe2O3) of 1:6 by mechanochemical synthesis process, followed by annealing… read more here.
Keywords: synthesis; synthesis time; magnetic properties; phase ... See more keywords
Luminescent properties of K2SbF5: Ln (Ln = Eu3+, Tb3+, Er3+) obtained by a facile room temperature mechanochemical synthesis
Sign Up to like & getrecommendations! Published in 2019 at "Journal of Luminescence"
DOI: 10.1016/j.jlumin.2019.02.061
Abstract: Abstract Mechanochemical synthesis of K2SbF5 by the successive grinding reactions of antimony (III) acetate with ammonium fluoride and potassium fluoride has been carried out. Powder X-ray diffraction pattern of K2SbF5 was refined successfully in orthorhombic… read more here.
Keywords: synthesis; luminescent properties; er3; properties k2sbf5 ... See more keywords