Continuous-/Micro-Flow Reactions Using Highly Electrophilic PCl3 and POCl3.
Sign Up to like & getrecommendations! Published in 2023 at "ChemPlusChem"
DOI: 10.1002/cplu.202300176
Abstract: PCl3 and POCl3 are the most important sources of phosphorus-containing compounds. They are also used for large-scale industrial productions. However, chemical reactions using the highly reactive PCl3 and POCl3 tend to result in overreactions. In… read more here.
Keywords: pcl3 pocl3; micro flow; pocl3; using highly ... See more keywords
A facile iron catalyzed cross-coupling reaction under micro-flow conditions
Sign Up to like & getrecommendations! Published in 2020 at "Journal of Flow Chemistry"
DOI: 10.1007/s41981-020-00091-9
Abstract: The iron-catalyzed cross-coupling reaction between an aromatic Grignard reagent and a haloalkane was investigated under micro-flow conditions. The reaction proceeded smoothly by the separate feeding of the substrate solutions to give the desired cross-coupling product.… read more here.
Keywords: iron catalyzed; micro flow; reaction; catalyzed cross ... See more keywords
Co and Ni extraction and separation in segmented micro-flow using a coiled flow inverter
Sign Up to like & getrecommendations! Published in 2017 at "Chemical Engineering Journal"
DOI: 10.1016/j.cej.2016.08.062
Abstract: The segmented micro-flow extraction and separation of the adjacent elements of Co from Ni sulphate solution with Cyanex 272 is developed using a micro-scale coiled flow inverter (CFI). This is compared with the conventional batch… read more here.
Keywords: extraction; extraction separation; micro flow; flow ... See more keywords
Deadzone compensation control based on detection of micro flow rate in pilot stage of proportional directional valve.
Sign Up to like & getrecommendations! Published in 2019 at "ISA transactions"
DOI: 10.1016/j.isatra.2019.03.030
Abstract: The pilot operated proportional directional valves (POPDVs) with a flow rate ranging from 100 to 1000 L/min are widely used in electro-hydraulic systems (EHSs). The deadzone of the pilot stage valve and its control compensation… read more here.
Keywords: flow rate; control; micro flow; pilot ... See more keywords
Analytical evaluation of a quadruple-mode micro-flow ultrasonic nebulizer for sample introduction in microwave induced plasma spectrometry
Sign Up to like & getrecommendations! Published in 2017 at "Microchemical Journal"
DOI: 10.1016/j.microc.2016.10.010
Abstract: Abstract The analytical potential of a coupled continuous-micro-flow ultrasonic nebulizer quadruple-mode micro-capillary system (μ-USN-QCS)-argon-helium microwave induced plasma-optical emission spectrometry (MIP-OES) has been evaluated for the purpose of determination of inorganic elements (Ba, Ca, Cd, Cu,… read more here.
Keywords: quadruple mode; flow ultrasonic; ultrasonic nebulizer; micro flow ... See more keywords
Quality-In(Process)Line (QuIProLi) process intensification for a micro-flow UV-photo synthesis enabled by online UHPLC analysis
Sign Up to like & getrecommendations! Published in 2018 at "Tetrahedron"
DOI: 10.1016/j.tet.2018.02.016
Abstract: Abstract Process intensification commonly enables reaction acceleration and therefore continuous-flow/PAT is urgently needed. The low volumes typical for micro-flow pose challenges for online sampling operations in analytics. In this paper, a very fast process is… read more here.
Keywords: quality; analysis; micro flow; process ... See more keywords
Robust Capillary- and Micro-Flow Liquid Chromatography-Tandem Mass Spectrometry Methods for High-Throughput Proteome Profiling.
Sign Up to like & getrecommendations! Published in 2022 at "Journal of proteome research"
DOI: 10.1021/acs.jproteome.2c00405
Abstract: Capillary- and micro-flow liquid chromatography-tandem mass spectrometry (capLC-MS/MS and μLC-MS/MS) is becoming a valuable alternative to nano-flow LC-MS/MS due to its high robustness and throughput. The systematic comparison of capLC-MS/MS and μLC-MS/MS systems for global… read more here.
Keywords: chromatography tandem; liquid chromatography; micro flow; flow ... See more keywords
Study on the performance of micro-flow injection preconcentration method on-line coupled to thermospray flame furnace AAS using MWCNTs wrapped with polyvinylpyridine nanocomposites as adsorbent
Sign Up to like & getrecommendations! Published in 2017 at "RSC Advances"
DOI: 10.1039/c7ra01220a
Abstract: This work describes the synthesis and characterization of a new adsorbent nanocomposite based on multi-walled carbon nanotubes (MWCNTs) and polyvinylpyridine and its use in the development of a highly sensitive micro-flow injection preconcentration method coupled… read more here.
Keywords: injection preconcentration; preconcentration method; flow injection; micro flow ... See more keywords
On the potential of micro-flow LC-MS/MS in proteomics
Sign Up to like & getrecommendations! Published in 2022 at "Expert Review of Proteomics"
DOI: 10.1080/14789450.2022.2134780
Abstract: ABSTRACT Introduction Due to its excellent sensitivity, nano-flow liquid chromatography tandem mass spectrometry (LC-MS/MS) is the mainstay in proteome research; however, this comes at the expense of limited throughput and robustness. In contrast, micro-flow LC-MS/MS… read more here.
Keywords: proteomic applications; micro flow; flow; proteomics potential ... See more keywords
Recent improvements of the French liquid micro-flow reference facility
Sign Up to like & getrecommendations! Published in 2018 at "Measurement Science and Technology"
DOI: 10.1088/1361-6501/aa97ef
Abstract: According to the mission of the national reference laboratory, LNE-CETIAT achieved in 2012 the construction and accreditation of a modern and innovative calibration laboratory based on the gravimetric method. The measurement capabilities cover a flow… read more here.
Keywords: flow rate; method; reference; micro flow ... See more keywords